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Synthesis and spectral analysis of 5,7-dihydroxy-3-(4-hydroxybenzyl)-6,8-dimethylchroman-4-one

By: Zhen, Lv.
Contributor(s): Yang, Jifang.
Publisher: New Delhi CSIR 2022Edition: Vol.61(8), Aug.Description: 866-869p.Subject(s): GENERAL CHEMISTRYOnline resources: Click here In: Indian journal of chemistry (Section B)Summary: An efficient and concise synthetic route was designed based on 5,7-dihydroxy-3-(4-hydroxybenzyl)-6,8-dimethylchroman-4-one, an important active ingredient extracted from PolygonatumOdoratum (Mill.) Druc. In this regard, spectroscopic techniques such as 1H and 13C NMR and high-resolution mass spectrometry (HRMS) were also performed to confirm the final structure. Also, microinfrared spectroscopy and micro-Raman spectroscopy were performed to further determine the structure of the compound.
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An efficient and concise synthetic route was designed based on 5,7-dihydroxy-3-(4-hydroxybenzyl)-6,8-dimethylchroman-4-one, an important active ingredient extracted from PolygonatumOdoratum (Mill.) Druc. In this regard, spectroscopic techniques such as 1H and 13C NMR and high-resolution mass spectrometry (HRMS) were also performed to confirm the final structure. Also, microinfrared spectroscopy and micro-Raman spectroscopy were performed to further determine the structure of the compound.

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